HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → N,N'-dibutyloxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Butylamine | HCID 8007 | — |
| Product | N,N'-dibutyloxamide | HCID 352186 | — |
Reaction Steps
The temperature is brought to 5° C. with an ice-bath and a solution of n-butyl-amine (25 ml, 0.253 mol) in anhydrous methyl alcohol (25 ml) is dripped in. The reaction is exothermic and dripping is adjusted to keep the temperature below 10°-12° C. When all the methyl alcohol solution of the amine has been added, the reaction mixture has a jelly appearance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04981963 |
| Source dataset | uspto-grants-1991_01 |
| ORD ID | ord-cd03387333f7441fa7bd71219a767b90 |
| Source note | uspto-grants-1991_01 |