huagongshe.com
HRID70329

反应详情

EQUATION

反应方程式

HRID 70329 的结构方程式

REACTANTS

反应物

2
结构：NC(=O)c1cccc(B(O)O)c1
HCID2737814

3-Aminocarbonylphenylboronic acid

C7H8BNO3

结构：FC(F)(F)c1cc(I)ccc1C1OCCO1
HCID58276681

未命名化合物

PRODUCTS

生成物

1
结构：NC(=O)c1cccc(-c2ccc(C3OCCO3)c(C(F)(F)F)c2)c1
HCID67159994

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO.Cc1ccccc1
溶剂HCID21863594

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 3-(aminocarbonyl)phenyl boronic acid and 2-[4-iodo-2-(trifluoromethyl)phenyl]-1,3-dioxolane (I-IX-7) according to the procedure described for IX-10, using PhMe/EtOH (4:1) as organic cosolvents. Colorless solid. LC/MS (method A) 2.38 min; m/z 338 (M+H).

WORKUP

后处理

  1. customLC/MS (method A) 2.38 min