Sodium Sulfate → HCID 19988348, compound
Reaction equation
[S:1]([O-:5])([O-:4])(=[O:3])=[O:2].[Al+3:6].[S:7]([O-:11])([O-:10])(=[O:9])=[O:8].[S:12]([O-:16])([O-:15])(=[O:14])=[O:13].[Al+3].S([O-])([O-])(=O)=O.[Na+:23].[Na+]>O>[S:1]([O-:5])([O-:4])(=[O:3])=[O:2].[S:7]([O-:11])([O-:10])(=[O:9])=[O:8].[S:12]([O-:16])([O-:15])(=[O:14])=[O:13].[Al+3:6].[Na+:23].[Na+:23].[Na+:23]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
In 5 liters of water were dissolved 291.5 g of aluminum sulfate [Al2 (SO4)3 13.4H2O] and 213.1 g of sodium sulfate [Na2SO4 ], and the solution was granulated and dried by the spray-drying method and the temperature of the granulation product contained in an alumina crucible having a capacity of 1 liter was elevated from room temperature at a rate of 10° C. per minute and heating reaction was carried out at 600° C. for 4 hours to obtain 384.2 g of trisodium aluminum trisulfate [Na3Al(SO4)3 ].
Workup
- customdried by the spray-drying method
- customwas elevated from room temperature at a rate of 10° C. per minute
- temperatureheating
- customreaction
Sources & evidence
- ORD record
- ord-70c3d778937b4db797e4a4240a9d19b3
- Source dataset
- uspto-grants-1991_01
- Patent number
- US04985222
Reaction notes
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