HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → HCID 54355381, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | HCID 53873990 | HCID 53873990 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 54355381 | HCID 54355381 | — |
Reaction Steps
A solution of methyl [1-(3-methoxyphenyl)hydrazino]acetate (1.6 g) and methyl isocyanate (0.9 ml) in acetonitrile (20 ml) was heated under reflux for 1 h. The solvent was removed in vacuo and the residue was treated with ether to give the title compound (1.8 g) as a solid, m.p. 145°-146°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04985427 |
| Source dataset | uspto-grants-1991_01 |
| ORD ID | ord-ed98e318cb954589b186d1d1e54d3a87 |
| Source note | uspto-grants-1991_01 |