HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → HCID 20074969, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 53808377 | HCID 53808377 | — |
| Product | HCID 20074969 | HCID 20074969 | — |
Reaction Steps
Methyl [1-[4-(phenylmethoxy)phenyl]hydrazino]acetate (0.73 g) was treated with methyl isocyanate (0.5 ml) and then with sodium methoxide solution (3.5 ml). The product was recrystallised from tetrahydrofuran-hexane to give the title compound (0.56 g), m.p. 224°-227°, t.l.c. (ethyl acetate) Rf 0.55.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04985427 |
| Source dataset | uspto-grants-1991_01 |
| ORD ID | ord-24ec6dd0ac4e41e598fa5e0b41630c98 |
| Source note | uspto-grants-1991_01 |