HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → HCID 14473602, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | (3-ethyl-1,2,4-oxadiazol-5-yl)methanamine | HCID 10820904 | — |
| Product | HCID 14473602 | HCID 14473602 | — |
Reaction Steps
A mixture of 26 g of 5-aminomethyl-3-ethyl-1,2,4-oxadiazole and 30 ml of dimethylformamide dimethylacetal is heated for 61/2 hours to 80° C. (bath temperature). Then 16 ml of methanol is distilled off and the formed product is purified by bulb tube distillation. 27.9 g (74.8%) of oil with a boiling point of 130°-150° C. (0.05 torr); nD20 : 1.4924.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04987146 |
| Source dataset | uspto-grants-1991_01 |
| ORD ID | ord-76eb1873a8774f84a50cd580ba33b84b |
| Source note | uspto-grants-1991_01 |