HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 4-styrylpiperidine-1carboxylate → Ethyl 4-(2-phenylethyl)piperidine-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 4-styrylpiperidine-1carboxylate | HCID 54197084 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Ethyl 4-(2-phenylethyl)piperidine-1-carboxylate | HCID 20074040 | 99.2% |
Reaction Steps
A mixture of 0.80 g of ethyl 4-styrylpiperidine-1carboxylate and 80 mg of 10% palladium-on-carbon in ethyl acetate (40 ml) was subjected to catalytic reduction at room temperature until stopping of hydrogen absorption. The catalyst was filtered off, and the filtrate was concentrated under reduced pressure to give 0.80 g of ethyl 4-(2-phenylethyl)piperidine-1-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04987132 |
| Source dataset | uspto-grants-1991_01 |
| ORD ID | ord-72ab2d8da791486eb82bc898cecd4a57 |
| Source note | uspto-grants-1991_01 |