HRID704385

反应详情

EQUATION

反应方程式

HRID 704385 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 0.80 g of ethyl 4-styrylpiperidine-1carboxylate and 80 mg of 10% palladium-on-carbon in ethyl acetate (40 ml) was subjected to catalytic reduction at room temperature until stopping of hydrogen absorption. The catalyst was filtered off, and the filtrate was concentrated under reduced pressure to give 0.80 g of ethyl 4-(2-phenylethyl)piperidine-1-carboxylate.

WORKUP

后处理

  1. customwas subjected to catalytic reduction at room temperature
  2. customuntil stopping of hydrogen absorption
  3. filtrationThe catalyst was filtered off
  4. concentrationthe filtrate was concentrated under reduced pressure