Hydrochloric Acid → HCID 20074096, compound

Participants

Reaction Steps

A solution of 580 mg of N-carboethoxy-N'-(3-phenylpropyl)ethylenediamine in 10 ml of concentrated hydrochloric acid was heated in a sealed tube at 120° C. overnight. The mixture was concentrated under reduced pressure. Toluene was added and the mixture was again concentrated. Two repetitions of this procedure gave 630 mg of N-(3-phenylpropyl)ethylenediamine dihydrochloride. This product was submitted to the next step without purification.

Provenance & Evidence