HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 4191957, compound → N-Butylpiperazine-1-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 4191957 | HCID 4191957 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-Butylpiperazine-1-carboxamide | HCID 20074044 | 116.8% |
Reaction Steps
10% Palladium-on-carbon (250 mg) was added to a solution of 2.8 g of 1-benzyl-4-butylaminocarbonylpiperazine in 15 ml of ethanol, and catalytic reduction was carried out until cessation of hydrogen absorption. The catalyst was then filtered off, and the filtrate was concentrated under reduced pressure to give 2.2 g of 1-butylaminocarbonylpiperazine. This product was submitted to the next step without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04987132 |
| Source dataset | uspto-grants-1991_01 |
| ORD ID | ord-4a3ab0ea5deb435d90e4711a1aa6fea4 |
| Source note | uspto-grants-1991_01 |