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HRID704574

反应详情

EQUATION

反应方程式

HRID 704574 的结构方程式

REACTANTS

反应物

2
结构：Cc1cc(O)ccc1N
HCID17819

4-Amino-m-cresol

C7H9NO

结构：ClCCc1nnc2ccccc2c1Cl
HCID20072752

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(O)ccc1N1CCc2nnc3ccccc3c21.Cl
HCID20072755

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

4-Chloro-3-(2-chloroethyl)cinnoline (1 g, 0.0044 mol) and 4-hydroxy-2-methylphenylamine (0.54 g, 0.0044 mol) in 1,4 dioxan (20 ml) were heated under reflux for 20 hours. The solid obtained was collected by filtration and dried. Recrystallization from ethanol gave the title compound, 0.4 g, m.p. >300°

WORKUP

后处理

  1. temperatureunder reflux for 20 hours
  2. customThe solid obtained
  3. filtrationwas collected by filtration
  4. customdried
  5. customRecrystallization from ethanol