Pyridine → HCID 86744552, compound

Participants

Reaction Steps

The product from step (a) (10.0 g) and hydroxylamine hydrochloride (7 g) were taken up in methanol (50 ml), pyridine (15 ml) was added and the mixture stirred for 1 hour. The mixture was then stripped, redissolved in ether, washed with 2N aqu. HCl and satd. aqu. NaCl, dried over MgSO4, and stripped to give the desired product (10.2 g).

Provenance & Evidence