HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(2,3-Epoxypropyl)phthalimide → HCID 13365967, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(2,3-Epoxypropyl)phthalimide | HCID 21601 | — |
| Reactant | HCID 4061276 | HCID 4061276 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 13365967 | HCID 13365967 | — |
Reaction Steps
0.022 mol of 2-(2,3-epoxypropyl)isoindole-1,3(2H)dione, 0.02 mol of 1-(5-(4-chlorophenyl)-2-pyrimidinyl)piperazine and 70 ml of isopropanol are heated to boiling for 2 hours. The mixture is evaporated and the residue is purified by column chromatography on silica gel 60. After elution with methylene chloride/alcohol (96:4), the compound is stirred with alcohol and filtered off with suction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04988809 |
| Source dataset | uspto-grants-1991_01 |
| ORD ID | ord-90bb8fb07ffd4f25b4cb974fde3177d1 |
| Source note | uspto-grants-1991_01 |