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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 704950Generated: October 31, 2026

Potassium Carbonate → HCID 13603078, compound

https://huagongshe.com/reaction/704950

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 20077950HCID 20077950—
ReactantHCID 178418642HCID 178418642—
SolventDimethylformamideHCID 6228—
ProductHCID 13603078HCID 13603078—

Reaction Steps

For instance, 4-hydroxypyridine is reacted with benzhydryl α-chloroacetate in a solvent such as N,N-dimethylformamide in the presence of potassium carbonate at a temperature of from 40° to 80° C. to form 1-benzhydryloxycarbonylmethyl-4-pyridone, followed by a reaction with phosphorus pentasulfide in a solvent such as tetrahydrofuran at a temperature of from 40° to 80° C. to obtain the product of the formula III.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04988687
Source datasetuspto-grants-1991_01
ORD IDord-35c0ab6ae58643688b64504ebbf7c4e1
Source noteuspto-grants-1991_01