HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 13603078, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 20077950 | HCID 20077950 | — |
| Reactant | HCID 178418642 | HCID 178418642 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 13603078 | HCID 13603078 | — |
Reaction Steps
For instance, 4-hydroxypyridine is reacted with benzhydryl α-chloroacetate in a solvent such as N,N-dimethylformamide in the presence of potassium carbonate at a temperature of from 40° to 80° C. to form 1-benzhydryloxycarbonylmethyl-4-pyridone, followed by a reaction with phosphorus pentasulfide in a solvent such as tetrahydrofuran at a temperature of from 40° to 80° C. to obtain the product of the formula III.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04988687 |
| Source dataset | uspto-grants-1991_01 |
| ORD ID | ord-35c0ab6ae58643688b64504ebbf7c4e1 |
| Source note | uspto-grants-1991_01 |