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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 705365Generated: October 29, 2026

O-(2,4,6-Trimethylbenzenesulfonyl)hydroxylamine → HCID 86710153, compound

https://huagongshe.com/reaction/705365

Reaction equation

Participants

RoleNameHCIDCharge
ReactantO-(2,4,6-Trimethylbenzenesulfonyl)hydroxylamineHCID 11830845—
ReactantHCID 86710155HCID 86710155—
SolventDichloromethaneHCID 6344—
ProductHCID 86710153HCID 86710153—

Reaction Steps

A solution of N-(4-cyclopropylpyridin-3-yl)-N-isopentylmethanesulfonamide (Example 17G, 474 mg, 1.68 mmol) in dichloromethane (3 mL) at 0° C. was treated with the solution of O-(mesitylsulfonyl)hydroxylamine (solution used directly from Example 17H). The solution was immediately warmed to room temperature and stirred for 1 hour. The solution was then used directly in Example 17K.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09173887B2
Source datasetuspto-grants-2015_11
ORD IDord-d574285215e14fcea7b27ec79c4e4f78
Source noteuspto-grants-2015_11