HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-(2,4,6-Trimethylbenzenesulfonyl)hydroxylamine → HCID 86710153, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-(2,4,6-Trimethylbenzenesulfonyl)hydroxylamine | HCID 11830845 | — |
| Reactant | HCID 86710155 | HCID 86710155 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86710153 | HCID 86710153 | — |
Reaction Steps
A solution of N-(4-cyclopropylpyridin-3-yl)-N-isopentylmethanesulfonamide (Example 17G, 474 mg, 1.68 mmol) in dichloromethane (3 mL) at 0° C. was treated with the solution of O-(mesitylsulfonyl)hydroxylamine (solution used directly from Example 17H). The solution was immediately warmed to room temperature and stirred for 1 hour. The solution was then used directly in Example 17K.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09173887B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-d574285215e14fcea7b27ec79c4e4f78 |
| Source note | uspto-grants-2015_11 |