HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 49856399, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 6-(1H-Imidazol-1-yl)-2-phenylquinazoline | HCID 24898732 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 49856399 | HCID 49856399 | — |
Reaction Steps
50 mg of 6-(1H-imidazol-1-yl)-2-phenylquinazoline are suspended in 2 mL of methanol, the suspension is heated at reflux for a few minutes, and then filtered and left to evaporate slowly at room temperature, at rest. The crystals obtained are analysed. XRPD: Form C. TGA: weight loss: 6.32% (theoretical value for C17H12N4.H2O: 6.2%), TGA-IR in agreement with the IR spectrum of H2O for the released vapours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09174966B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-61d7491b00d641fcaf4e6c9f0042903d |
| Source note | uspto-grants-2015_11 |