HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thioglycolic Acid → HCID 86652688, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thioglycolic Acid | HCID 1133 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 5-Aminobenzimidazole | HCID 13623 | — |
| Reactant | 4-Fluorobenzaldehyde | HCID 68023 | — |
| Product | HCID 86652688 | HCID 86652688 | — |
Reaction Steps
The compound was synthesized starting from 5-aminobenzimidazole (0.133 g, 1.0 mmol), 4-fluoro-benzaldehyde (0.108 mL, 1.0 mmol), mercapto acetic acid (0.138 g, 1.5 mmol), piperidine, according to method 9 step A. yield: 69 mg (22%), MS m/z: 314.3 (M+H)+, HPLC [A]): rt 5.86 min (97%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09173885B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-1bdb65d433ce4dc5a661b5bdb3cd75d1 |
| Source note | uspto-grants-2015_11 |