HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thioglycolic Acid → HCID 51030404, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thioglycolic Acid | HCID 1133 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 5-Aminobenzimidazole | HCID 13623 | — |
| Product | HCID 51030404 | HCID 51030404 | — |
Reaction Steps
The compound was synthesized starting from 5-aminobenzimidazole (0.133 g, 1.0 mmol), 4-naphthalen-1-yl carbaldehyde (0.157 mL, 1.0 mmol), mercapto acetic acid (0.157 g, 1.5 mmol), piperidine, according to method 9 step A yield: 54 mg (15.6%), MS m/z: 346.3 (M+H)+, HPLC [A]): rt 6.86 min (95%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09173885B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-21ef71a82b7d4034bbdf71e00841c5ab |
| Source note | uspto-grants-2015_11 |