HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thioglycolic Acid → HCID 51030405, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thioglycolic Acid | HCID 1133 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 5-Aminobenzimidazole | HCID 13623 | — |
| Reactant | 2,6-Difluorobenzaldehyde | HCID 136284 | — |
| Product | HCID 51030405 | HCID 51030405 | — |
Reaction Steps
The compound was synthesized starting from 5-aminobenzimidazole (0.133 g, 1.0 mmol), 2,6-difluoro-benzaldehyde (0.142 mg, 1.0 mmol), mercapto acetic acid (0.157 g, 1.5 mmol), piperidine, according to method 9 step A. yield: 208 mg (62.8%), MS m/z: 332.3 (M+H)+, HPLC [A]): rt 5.76 min (97%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09173885B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-f82e7378d7b047a9a91c6a28b555a6ab |
| Source note | uspto-grants-2015_11 |