HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13314942, compound → HCID 58046553, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13314942 | HCID 13314942 | — |
| Reactant | HCID 58046554 | HCID 58046554 | — |
| Product | HCID 58046553 | HCID 58046553 | 64% |
Reaction Steps
Alkylation of 1-(2-chloropyridin-4-yl)carbonyl-5-chloro-spiro[indolin-3,4′-piperidine] (0.18 g) with 1-chloro-4-((Z)-1,3-dichloro-propenyl)-benzene obtained in step 3 (0.11 g) was carried out following the procedure described in example 101, step 4 to afford 0.17 g of the title compound (64%) as a foam which was characterized by its mass and NMR spectra. MS (ES+) 548.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09174987B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-7b2185daaeba48379775b3f63ead26a9 |
| Source note | uspto-grants-2015_11 |