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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 706574Generated: October 30, 2026

HCID 86699326, compound → HCID 15050249, compound

https://huagongshe.com/reaction/706574

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86699326HCID 86699326—
ReactantHCID 178418361HCID 178418361—
CatalystPalladium hydroxideHCID 9942167—
SolventMethanolHCID 887—
ProductHCID 15050249HCID 1505024984%

Reaction Steps

5-(prop-1-en-2-yl)picolinaldehyde (0.600 g, 4.08 mmol) was dissolved in methanol (15 mL). To this was added Pd(OH)2 (0.600 mgs, 20% catalyst on carbon, 50% water by weight) and the mixture was hydrogenated under a balloon of hydrogen for 2 hours. The mixture was then filtered through GF/F filter paper and the filtrate was concentrated under reduced pressure to give the title compound (84%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09174981B2
Source datasetuspto-grants-2015_11
ORD IDord-5fca247aee1242bc8139b12a8059d713
Source noteuspto-grants-2015_11