HRID707052

反应详情

EQUATION

反应方程式

HRID 707052 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of morpholine-4-carbonyl chloride (2.0 g) in methanol (10 mL) and 7 N NH3 in methanol (5 mL) was stirred at 45° C. overnight. The mixture was concentrated to give a solid, which was dried under vacuum.

WORKUP

后处理

  1. concentrationThe mixture was concentrated
  2. customto give a solid, which
  3. customwas dried under vacuum