HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → Morpholine-4-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 4-Morpholinecarbonyl chloride | HCID 84810 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Morpholine-4-carboxamide | HCID 75088 | — |
Reaction Steps
A solution of morpholine-4-carbonyl chloride (2.0 g) in methanol (10 mL) and 7 N NH3 in methanol (5 mL) was stirred at 45° C. overnight. The mixture was concentrated to give a solid, which was dried under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09174982B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-2ae19c97422d4561a7a7cd351007e089 |
| Source note | uspto-grants-2015_11 |