Hydrochloric Acid → HCID 178426488, compound

Participants

Reaction Steps

To a round bottomed flask was added tert-butyl(cis-4-((5-methylpyridin-2-yl)amino)cyclohexyl)carbamate (0.2795 g, 0.915 mmol) and hydrogen chloride, 4.0M solution in 1,4-dioxane (1.144 ml, 4.58 mmol, Sigma-Aldrich Chemical Company, Inc.) to stir at room temperature for 6 h. Solvent was evaporated in vacuo to provide the title compound, which was carried on without further work up. LCMS showed product peak at 0.357 min (m+1=206.0).

Provenance & Evidence