HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 86706842, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 2-Methylpyrimidine-5-carbaldehyde | HCID 3160970 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86706842 | HCID 86706842 | — |
Reaction Steps
As per scheme-4, 2-methyl-pyrimidine-5-carbaldehyde (4-a) is reacted with hydroxylamine hydrochloride in the presence of base such as sodium carbonate or sodiumbicarbonate or potassium carbonate in a suitable solvent such as methanol or ethanol or water or mixture thereof, at a temperature ranging from 0° C. to 35° C., to provide corresponding 2-methyl-pyrimidine-5-carbaldehyde oxime (4-b).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09175031B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-ba58cf9a874c41deb67fe1e3e54e363d |
| Source note | uspto-grants-2015_11 |