Hydrochloric Acid → HCID 118098709, compound

Participants

Reaction Steps

10D (115 mg, 0.255 mmol) was dissolved in MeOH (5 mL) containing HCl (93 mg, 2.55 mmol). 10% Pd/C was added. The reaction mixture was stirred under a hydrogen balloon for 12 h. Pd/C was removed by filtration and the filtrate was concentrated under reduced pressure to give 10E (93 mg, 0.259 mmol, 101% yield).

Provenance & Evidence