HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 178443076, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | N-Palmitoylglycine | HCID 151008 | — |
| Reactant | HCID 178419078 | HCID 178419078 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 178443076 | HCID 178443076 | — |
Reaction Steps
Using thionyl chloride, N-palmitoyl-Gly was converted to the acid chloride in toluene at room temperature, then reacted with L-histidine using triethylamine as the base. However, only a trace amount of N-palmitoyl-Gly-His formed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09180201B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-3b47184941904363ac92444c72623d0e |
| Source note | uspto-grants-2015_11 |