huagongshe.com
HRID709328

反应详情

EQUATION

反应方程式

HRID 709328 的结构方程式

REACTANTS

反应物

4
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

结构：CCCCCCCCCCCCCCCC(=O)NCC(=O)O
HCID151008

N-Palmitoylglycine

C18H35NO3

结构：N[C@@H](Cc1c[nH]cn1)C(=O)O
HCID178419078

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCCCCCCCCCCC(=O)NCC(=O)N[C@@H](Cc1c[nH]cn1)C(=O)O
HCID178443076

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1
溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

Using thionyl chloride, N-palmitoyl-Gly was converted to the acid chloride in toluene at room temperature, then reacted with L-histidine using triethylamine as the base. However, only a trace amount of N-palmitoyl-Gly-His formed.