1,2-Dichloropropane → 1-Decene

HRID 709338Notes

Reaction equation

HRID 709338 reaction equation
Cl[CH2:2][CH:3](Cl)[CH3:4].[CH2:6]([CH:8]1O[CH2:9]1)Cl.[CH3:11][C:12](=[CH:15][CH2:16]C)C=O>>[CH2:4]=[CH:3][CH2:2][CH2:6][CH2:8][CH2:9][CH2:11][CH2:12][CH2:15][CH3:16]

Participants

4

Reactant 3

HCID 65641,2-DichloropropaneHCID 7835EpichlorohydrinHCID 121772-Methyl-2-pentenal

Product 1

HCID 133811-Decene

Procedure

Column 2 separates the lighter boiling 1,2-dichloropropane, residual epichlorohydrin, and 2-methyl-2-pentenal in the overheads and obtains 1-decene and DCP at the bottom. Stream details for Column 2 are shown in Table 5.

Sources & evidence

ORD record
ord-9b8e273166854e7c93a4bb2ee531ac99
Source dataset
uspto-grants-2015_11
Patent number
US09180384B2

Reaction notes

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