HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 709341Generated: October 29, 2026
4-Methylbenzylamine → HCID 523206, compound
https://huagongshe.com/reaction/709341
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Methylbenzylamine | HCID 66035 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 523206 | HCID 523206 | 82% |
Reaction Steps
4-Methylbenzylamine (0.5 mmol) was also heated with catalyst Pd@ba-GO (10 mg) and solvent CH3CN (0.2 mL) at 90° C. in a flask open to air for 6 hours, and then stirred also at 90° C. under H2 gas (1 atm) for 8 hours to obtain di-(4-methylbenzyl)amine. Again, an unexpectedly high yield of 82% was achieved.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09180442B2 |
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| Source dataset | uspto-grants-2015_11 |
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| ORD ID | ord-f4eb36fc90ee4560b2c729e81e8b1ad6 |
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| Source note | uspto-grants-2015_11 |
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