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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 709341Generated: October 29, 2026

4-Methylbenzylamine → HCID 523206, compound

https://huagongshe.com/reaction/709341

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-MethylbenzylamineHCID 66035—
CatalystPalladiumHCID 23938—
SolventAcetonitrileHCID 6342—
ProductHCID 523206HCID 52320682%

Reaction Conditions

Temperature90 °C

Reaction Steps

4-Methylbenzylamine (0.5 mmol) was also heated with catalyst Pd@ba-GO (10 mg) and solvent CH3CN (0.2 mL) at 90° C. in a flask open to air for 6 hours, and then stirred also at 90° C. under H2 gas (1 atm) for 8 hours to obtain di-(4-methylbenzyl)amine. Again, an unexpectedly high yield of 82% was achieved.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09180442B2
Source datasetuspto-grants-2015_11
ORD IDord-f4eb36fc90ee4560b2c729e81e8b1ad6
Source noteuspto-grants-2015_11