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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 709342Generated: October 28, 2026

3-Methylbenzylamine → HCID 10785436, compound

https://huagongshe.com/reaction/709342

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-MethylbenzylamineHCID 66015—
CatalystPalladiumHCID 23938—
SolventAcetonitrileHCID 6342—
ProductHCID 10785436HCID 1078543690%

Reaction Conditions

Temperature90 °C

Reaction Steps

3-Methylbenzylamine (0.5 mmol) was heated with catalyst Pd@ba-GO (10 mg) and solvent CH3CN (0.2 mL) at 90° C. in a flask open to air for 6 hours, and then stirred also at 90° C. under H2 gas (1 atm) for 8 hours to obtain di-(3-methylbenzyl)amine. An unexpectedly high yield of 90% was observed.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09180442B2
Source datasetuspto-grants-2015_11
ORD IDord-25751c398aed468893b5bca764be17b4
Source noteuspto-grants-2015_11