HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 709342Generated: October 28, 2026
3-Methylbenzylamine → HCID 10785436, compound
https://huagongshe.com/reaction/709342
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3-Methylbenzylamine | HCID 66015 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 10785436 | HCID 10785436 | 90% |
Reaction Steps
3-Methylbenzylamine (0.5 mmol) was heated with catalyst Pd@ba-GO (10 mg) and solvent CH3CN (0.2 mL) at 90° C. in a flask open to air for 6 hours, and then stirred also at 90° C. under H2 gas (1 atm) for 8 hours to obtain di-(3-methylbenzyl)amine. An unexpectedly high yield of 90% was observed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09180442B2 |
|---|
| Source dataset | uspto-grants-2015_11 |
|---|
| ORD ID | ord-25751c398aed468893b5bca764be17b4 |
|---|
| Source note | uspto-grants-2015_11 |
|---|