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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 709343Generated: October 29, 2026

2-Methylbenzylamine → HCID 19843001, compound

https://huagongshe.com/reaction/709343

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-MethylbenzylamineHCID 6993—
CatalystPalladiumHCID 23938—
SolventAcetonitrileHCID 6342—
ProductHCID 19843001HCID 1984300187%

Reaction Conditions

Temperature90 °C

Reaction Steps

2-Methylbenzylamine (0.5 mmol) was heated with catalyst Pd@ba-GO (10 mg) and solvent CH3CN (0.2 mL) at 90° C. in a flask open to air for 6 hours, and then stirred also at 90° C. under H2 gas (1 atm) for 6 hours to obtain di-(2-methylbenzyl)amine. Again, an unexpectedly high yield of 87% was observed.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09180442B2
Source datasetuspto-grants-2015_11
ORD IDord-8a636c60851447e3bb89c28e9fd60123
Source noteuspto-grants-2015_11