HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 709343Generated: October 29, 2026
2-Methylbenzylamine → HCID 19843001, compound
https://huagongshe.com/reaction/709343
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Methylbenzylamine | HCID 6993 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 19843001 | HCID 19843001 | 87% |
Reaction Steps
2-Methylbenzylamine (0.5 mmol) was heated with catalyst Pd@ba-GO (10 mg) and solvent CH3CN (0.2 mL) at 90° C. in a flask open to air for 6 hours, and then stirred also at 90° C. under H2 gas (1 atm) for 6 hours to obtain di-(2-methylbenzyl)amine. Again, an unexpectedly high yield of 87% was observed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09180442B2 |
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| Source dataset | uspto-grants-2015_11 |
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| ORD ID | ord-8a636c60851447e3bb89c28e9fd60123 |
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| Source note | uspto-grants-2015_11 |
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