Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Isatin | HCID 7054 | — |
| Reactant | 4-Methoxyphenylacetic Acid | HCID 7690 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Product | HCID 68767389 | HCID 68767389 | — |
Reaction Steps
7.5 mmol of isatin (III), 1.875 mmol of sodium acetate, and 13.125 mmol p-methoxyphenylacetic acid were mixed, heated to 150-200° C. and refluxed for 1-5 h. The reaction was finished by TLC detection. The reaction solution was washed with petroleum ether and acetone successively. After separated by column chromatography, the title compound was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09181193B2 |
|---|
| Source dataset | uspto-grants-2015_11 |
|---|
| ORD ID | ord-ec545ff4112c46a3acc19e617e8c754c |
|---|
| Source note | uspto-grants-2015_11 |
|---|
