HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 117760086, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 117760087 | HCID 117760087 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 117760086 | HCID 117760086 | 56.2% |
Reaction Steps
To a solution of 3-(3-((6-(2,2-dimethylpropyl)-5-(2-fluoro-5-methoxyphenyl)pyridin-2-yl)methoxy)-5-methylphenyl)propanoic acid (259 mg) in methanol (5.0 mL) was added sodium methoxide (29 mg) at room temperature, and the mixture was stirred for 1 hr. The reaction mixture was concentrated under reduced pressure. The residue was washed with hexane, and dried to give the title compound (147 mg) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181186B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-ea4f58dd2e6d4533a74394e3424c2495 |
| Source note | uspto-grants-2015_11 |