HRID710167

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CNC(=O)c1ccc(B2OC(C)(C)C(C)(C)O2)cc1C

HCID57516536

未命名化合物

结构：CC(C)OC(=O)N1CCC(c2nc3cc(Br)ccc3o2)CC1

HCID71257568

未命名化合物

PRODUCTS

生成物

结构：CNC(=O)c1ccc(-c2ccc3oc(C4CCN(C(=O)OC(C)C)CC4)nc3c2)cc1C

HCID71257368

未命名化合物

收率 10.1%

PROCEDURE

实验过程

Following the General Procedure-3, the titled compound (30 mg) was prepared from Intermediate 13 (250 mg, 0.68 mmol) and N,2-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide (187 mg, 0.68 mmol) as an off-white solid. M.P.: 151-154° C. MS (m/z): 436.5 [M+H]+.