N,2-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide → HCID 71257368, compound

Participants

Role	Name	HCID	Charge
Reactant	N,2-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide	HCID 57516536	—
Reactant	Isopropyl 4-(5-bromobenzo[d]oxazol-2-yl)piperidine-1-carboxylate	HCID 71257568	—
Product	HCID 71257368	HCID 71257368	10.1%

Reaction Steps

Following the General Procedure-3, the titled compound (30 mg) was prepared from Intermediate 13 (250 mg, 0.68 mmol) and N,2-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide (187 mg, 0.68 mmol) as an off-white solid. M.P.: 151-154° C. MS (m/z): 436.5 [M+H]+.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US09181214B2
Source dataset	uspto-grants-2015_11
ORD ID	ord-bf84b4addef54f46b85c7107d4ffa212
Source note	uspto-grants-2015_11