HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 710248Generated: October 29, 2026
4-Fluorobenzohydrazide → HCID 178452467, compound
https://huagongshe.com/reaction/710248
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Fluorobenzohydrazide | HCID 9972 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | tert-butyl (2S)-2-(4-cyanophenyl)morpholine-4-carboxylate | HCID 66861409 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 178452467 | HCID 178452467 | — |
Reaction Steps
4-Fluorobenzhydrazide (50 mg, 0.324) an (S)-tert-butyl 2-(4-cyanophenyl)morpholine-4-carboxylate (112 mg, 0.389 mmol) and potassium carbonate (22.5 mg, 0.162 mmol) was dissolved in butan-1-ol (1 ml) and stirred in a closed vial for 3 h at 150° C. The vial was opened and heating was continued for another 15 min to evaporate most of the solvent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09181230B2 |
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| Source dataset | uspto-grants-2015_11 |
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| ORD ID | ord-0aeace0f06fc4708ae2f804f08c05246 |
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| Source note | uspto-grants-2015_11 |
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