tert-Butyl 2,2-dimethyl-5-((4-octylphenylamino)methyl)-1,3-dioxan-5-ylcarbamate → HCID 46195743, compound

Participants

Reaction Steps

When the product of Step F was substituted for tert-butyl 2,2-dimethyl-5-((4-octylphenylamino)methyl)-1,3-dioxan-5-yl-carbamate in Example 1, Step B, the identical process afforded the title compound in 48% yield., as creamy paste. 1H-NMR (CDCl3) 0.87 (tr, 3H, J=6.93 Hz); 1.12-1.28 (m, 12H); 2.5 (tr, 2H, J=7.77 Hz); 2.59 (s, 2H); 2.76-2.83 (m, 8H); 3.52 (s, 4H); 6.78-6.94 (m, 3H).

Provenance & Evidence