HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → HCID 178420321, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | HCID 58433284 | HCID 58433284 | — |
| Product | HCID 178420321 | HCID 178420321 | — |
Reaction Steps
The compound was synthesized starting from 5-(1,3,4-oxadiazol-2-yl)benzimidazole (186 mg, 1 mmol) and benzylamine (0.5 ml) as described above; yield: 0.072 g (26.2%); MS m/z: 276.5 [M+H]+; 1H-NMR (DMSO d6, 400 MHz): δ 5.39 (s, 2H); 6.99-7.01 (m, 2H); 7.20-7.29 (m, 3H); 7.63 (dd, 1H, 4J=1.7 Hz, 3J=8.7 Hz); 7.83 (d, 1H, 3J=8.7 Hz); 7.93 (br s, 1H); 8.79 (s, 1H); 9.09 (s, 1H); HPLC (METHOD [A]): rt 7.81 min (100%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181233B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-1ea213e7683440a0afd9deb4089a2552 |
| Source note | uspto-grants-2015_11 |