Veratrylamine → HCID 178490831, compound

Participants

Reaction Steps

The compound was synthesized starting from 5-(1,3,4-oxadiazol-2-yl)benzimidazole (186 mg, 1 mmol) and 3,4-Dimethoxybenzylamine (0.5 ml) as described above; yield: 0.087 g (25.9%); MS m/z: 336.3 [M+H]+; 1H-NMR (DMSO d6, 400 MHz): δ 3.55 (s, 3H); 3.65 (s, 3H); 5.27 (s, 2H); 6.50 (dd, 1H, 4J=2.1 Hz, 3J=8.3 Hz); 6.64 (d, 1H, 4J=2.1 Hz); 6.81 (d, 1H, 3J=8.3 Hz), 7.62 (dd, 1H, 4J=1.2 Hz, 3J=8.7 Hz); 7.83 (d, 1H, 3J=8.7 Hz); 7.92 (br s, 1H); 8.76 (s, 1H); 8.98 (s, 1H); HPLC (METHOD [A]): rt 7.36 min (100%)

Provenance & Evidence