4-Methoxybenzylamine → HCID 178490830, compound

Participants

Reaction Steps

The compound was synthesized starting from 5-(1,3,4-oxadiazol-2-yl)benzimidazole (186 mg, 1 mmol) and 4-methoxybenzylamine (0.5 ml) as described above; yield: 0.083 g (27.2%); MS m/z: 306.4 [M+H]+; 1H-NMR (DMSO d6, 400 MHz): δ 3.66 (s, 3H); 5.29 (s, 2H); 6.80-6.83 (m, 2H); 6.95-6.97 (m, 2H); 7.61 (dd, 1H, 4J=1.7 Hz, 3J=8.7 Hz); 7.82 (d, 1H, 3J=8.7 Hz); 7.91 (d, 1H, 4J=1.7 Hz); 8.73 (s, 1H); 8.96 (s, 1H); HPLC (METHOD [A]): it 8.18 min (99.6%)

Provenance & Evidence