HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenepropanoyl chloride → HCID 178420224, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenepropanoyl chloride | HCID 64801 | — |
| Reactant | Lawesson's reagent | HCID 87949 | — |
| Reactant | 1H-benzimidazole-5-carbohydrazide | HCID 16637119 | — |
| Product | HCID 178420224 | HCID 178420224 | — |
Reaction Steps
The compound was synthesized starting from benzimidazol-5-carbohydrazide (176 mg; 1 mmol), TEA (0.153 ml; 1.1 mmol), phenylpropionylchloride (0.163 ml; 1.1 mmol) and Lawesson's reagent (606 mg; 1.5 mmol) as described in method 1; yield: 0.067 g (21.9%);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181233B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-76963735055f4f58b8e2d866a410974c |
| Source note | uspto-grants-2015_11 |