HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 178492790, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | Lawesson's reagent | HCID 87949 | — |
| Reactant | 2-(3,4-Dimethoxyphenylthio)acetic acid | HCID 725038 | — |
| Reactant | 1H-benzimidazole-5-carbohydrazide | HCID 16637119 | — |
| Product | HCID 178492790 | HCID 178492790 | — |
Reaction Steps
The compound was synthesized starting from (3,4-dimethoxyphenylthio)acetic acid (229 mg; 1 mmol), benzimidazol-5-carbohydrazide (176 mg; 1 mmol), Lawesson's reagent (606 mg; 1.5 mmol) and POCl3 (0.137 ml; 1.5 mmol) as described in method 3; yield: 0.042 g (10.9%);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181233B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-2452105ab5d94164a290b7480bd7cd96 |
| Source note | uspto-grants-2015_11 |