m-Chloroperbenzoic acid → HCID 72700242, compound

Participants

Reaction Steps

N-cyclopropyl-4-oxo-1-[3-(pyridin-3-ylethynyl)phenyl]-1,4-dihydropyridino[2,3-c]p yridazine-3-formamide (0.15 g, 0.36 mmol) was dissolved in 50 mL of dichloromethane solution, m-chloroperoxybenzoic acid (0.062 g, 0.36 mmol) was added and reacted at room temperature. After reaction was complete, separation was purified by liquid preparation chromatography column to obtain product 27 mg.

Provenance & Evidence