Hydrazine, (4-chlorophenyl)-, hydrochloride (1:1) → HCID 57876071, compound

HRID 710779Notes

Reaction equation

HRID 710779 reaction equation
Br[CH2:2][CH2:3][N:4]1[CH2:8][CH2:7][C:6]([CH3:10])([CH3:9])[CH2:5]1.Cl.[Cl:12][C:13]1[CH:18]=[CH:17][C:16]([NH:19]N)=[CH:15][CH:14]=1.[CH3:21][N:22]1[CH2:27][CH2:26][C:25](=O)[CH2:24][CH2:23]1>C(N(CC)CC)C>[Cl:12][C:13]1[CH:18]=[CH:17][C:16]2[N:19]([CH2:2][CH2:3][N:4]3[CH2:8][CH2:7][C:6]([CH3:10])([CH3:9])[CH2:5]3)[C:25]3[CH2:26][CH2:27][N:22]([CH3:21])[CH2:23][C:24]=3[C:15]=2[CH:14]=1

Participants

5

Reactant 3

HCID 71600Hydrazine, (4-chlorophenyl)-, hydrochloride (1:1)HCID 740491-Methyl-4-piperidoneHCID 68731855HCID 68731855, compound

Product 1

HCID 57876071HCID 57876071, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

The title compound is prepared by following Method 8 by using 1-(2-bromoethyl)-3,3-dimethylpyrrolidine, 4-chlorophenylhydrazine hydrochloride, triethylamine and N-methyl-4-piperidone

Sources & evidence

ORD record
ord-95b5d3e2e99c4bfd9ebf0e62a3fb8936
Source dataset
uspto-grants-2015_11
Patent number
US09181240B2

Reaction notes

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