HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosulfamic acid → HCID 67400524, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosulfamic acid | HCID 24499 | — |
| Reactant | 4-Amino-3-cyanobenzotrifluoride | HCID 12627361 | — |
| Product | HCID 67400524 | HCID 67400524 | — |
Reaction Steps
Prepared as in Example 77a from 2-amino-5-(trifluoromethyl)benzonitrile (Example 86b) and sulfamoyl chloride. 1H NMR (400 MHz, DMSO-d6) δ 7.53 (s, 2H), 7.74-7.76 (d, J=8.4 Hz, 1H), 8.01-8.03 (dd, J=8.4 Hz, 1.6 Hz, 1H), 8.23-8.233 (d, J=1.2 Hz, 1H), 10.16 (b, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181276B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-305883dec0aa4c4fbe575b37048cd825 |
| Source note | uspto-grants-2015_11 |