HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Pentanol → HCID 67400135, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Pentanol | HCID 11428 | — |
| Reactant | Dinitrobenzonitrile | HCID 520718 | — |
| Product | HCID 67400135 | HCID 67400135 | 86.5% |
Reaction Steps
Prepared as in Example 111c from pentan-3-ol and 2,6-dinitrobenzonitrile in 86.5% yield. 1H NMR (400 MHz, DMSO-d6) δ 0.94 (t, J=7.6 Hz, 6H), 1.70 (m, 4H), 4.62 (m, 1H), 7.78 (dd, J=7.2, 2.4 Hz, 1H), 7.88 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181276B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-2894cfd4686a4ed0ac8c844231839cc3 |
| Source note | uspto-grants-2015_11 |