HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxy-1-propanol → HCID 67400006, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxy-1-propanol | HCID 74116 | — |
| Reactant | Dinitrobenzonitrile | HCID 520718 | — |
| Product | HCID 67400006 | HCID 67400006 | 63.6% |
Reaction Steps
Prepared as in Example 111c from 3-methoxypropan-1-ol and 2,6-dinitrobenzonitrile in 63.6% yield. 1H NMR (400 MHz, CDCl3) δ 2.16 (m, 2H), 3.36 (s, 3H), 3.63 (t, J=5.6 Hz, 2H), 4.29 (t, J=6.4 Hz, 2H), 7.35 (dd, J=8.8, 0.8 Hz, 1H), 7.69 (t, J=8.8 Hz, 1H), (dd, J=8.4, 0.8 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181276B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-d7a45cdfd29a43c9a04925e31811d176 |
| Source note | uspto-grants-2015_11 |