HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 67398744, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 67401355 | HCID 67401355 | — |
| Product | HCID 67398744 | HCID 67398744 | 66% |
Reaction Steps
Prepared as in Example 231c from 2-(3-hydroxy-2,2-dimethylpropoxy)-6-nitrobenzonitrile (Example 233d) and acetyl chloride in 66% yield. 1H NMR (400 MHz, DMSO-d6) δ 1.04 (s, 6H), 2.00 (s, 3H), 3.95 (s, 2H), 4.02 (s, 2H), 7.70-7.72 (m, 1H), 7.85-7.92 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181276B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-a31a330b3097473198ca4933ce0ad410 |
| Source note | uspto-grants-2015_11 |