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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 711868Generated: November 2, 2026

Butanethiol → HCID 67399977, compound

https://huagongshe.com/reaction/711868

Reaction equation

Participants

RoleNameHCIDCharge
ReactantButanethiolHCID 8012—
ReactantDinitrobenzonitrileHCID 520718—
ProductHCID 67399977HCID 6739997790%

Reaction Steps

Prepared as in Example 215c from butane-1-thiol and 2,6-dinitrobenzonitrile in 90% yield. 1H NMR (400 MHz, CDCl3) δ 0.97 (t, J=7.2 Hz, 3H), 1.42-1.55 (m, 2H), 1.70-1.77 (m, 2H), 3.09 (t, J=7.2 Hz, 2H), 7.63-7.69 (m, 2H), 7.99-8.01 (m, 1H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09181276B2
Source datasetuspto-grants-2015_11
ORD IDord-e223a3d67fe544cc8a96cce51adec3d7
Source noteuspto-grants-2015_11